CN101411522A - Method for preparing dried sea-cucumber of ultra-high pressure - Google Patents
Method for preparing dried sea-cucumber of ultra-high pressure Download PDFInfo
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- CN101411522A CN101411522A CNA2008101621742A CN200810162174A CN101411522A CN 101411522 A CN101411522 A CN 101411522A CN A2008101621742 A CNA2008101621742 A CN A2008101621742A CN 200810162174 A CN200810162174 A CN 200810162174A CN 101411522 A CN101411522 A CN 101411522A
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Abstract
The invention discloses a method for preparing dried sea cucumber through extra high pressure, which comprises the following steps: sea cucumber preprocessing, ion compounding, protective liquid compound preparation, extra high pressure technical processing, circulatory drying, and nitrogen-charged packaging. The method can better keep the components of glycosaminoglycan and fucoidin in the sea cucumber body, simultaneously has the effects of sterilization and enzyme killing, improves the quality safety of the sea cucumber under normal state, and can effectively preserve the natural nutrient content of the sea cucumber body; beside, the produced sea cucumber has the characteristics of original color, original nutrition, low water content, moisture regain resistance, salt uprising resistance, and deformation resistance.
Description
Technical field
The present invention relates to a kind of preparation method of dried sea-cucumber of ultra-high pressure.
Background technology
The structure of glycosaminoglycan extracted from sea cucumber in the sea cucumber body wall and sea cucumber fucoidin is special to be that sea cucumber is distinctive, and its content is abundant, and sea cucumber is called as " rich polyanion food ".But processing sea cucumber is produced in the high-temperature region all the time for a long time, makes sea cucumber polysaccharide be subjected to serious loss.Through sea cucumber polyanion composition The Characteristic Study is confirmed; Sea cucumber has antitumor action, improves immunity of organisms, and anti-new vessels forms, and is a kind of novel anti-coagulants, promotes Fibrinolytic ability, reduces WBV and plasma viscosity effect, promotes body in effects such as blood functional rehabilitations.Traditional sea cucumber is adopted high-temperature processing technology, glycosaminoglycan and fucoidin composition in the prepared sea cucumber body obviously reduce, do not possess sterilization, the enzyme effect of going out, and can not effectively keep sea cucumber polyanion composition characteristic, and to boil water repeatedly of conventional processing sea cucumber, add thermal maturation again and caused sea cucumber polysaccharide and protein loss phenomenon, the natural nutritional labeling that can't effectively preserve the sea cucumber body.
Summary of the invention
The object of the present invention is to provide a kind of preparation method of dried sea-cucumber of ultra-high pressure, the present invention can better keep glycosaminoglycan and the fucoidin composition in the sea cucumber body, have sterilization simultaneously, the enzyme effect of going out strengthens the security of quality under the sea cucumber normality, can effectively preserve the natural nutritional labeling of sea cucumber body, and the sea cucumber that produces has former color and luster, former nutrition, and moisture is low, anti-moisture regain, the anti-accumulation of salt in the surface soil, the characteristics of resistance type.
In order to achieve the above object, technical scheme of the present invention is:
A kind of preparation method of dried sea-cucumber of ultra-high pressure, finished by following step:
(1) sea cucumber preprocessing: cut fresh and alive sea cucumbers the openning of 15-25mm open in the middle of the belly, reject internal organ, clean up, be seated in 16 ℃-18 ℃ the drinkable water and soak desalination 6-10h, pull out to drench and do.
(2) compound ion: adopt the Stainless Steel Vacuum reactor, pretreated sea cucumber is thrown in reactor, add sea cucumber weight 1:2-3 2-4% sulfuric acid dextran solution doubly, at vacuum 100pa-200pa, 40 ℃-60 ℃ of temperature, carried out the compound 4-6 of anion hour, and removed vacuum again, the taking-up sea cucumber is standby.
(3) composite protection liquid: adopt the protection liquid A of shitosan and sodium phosphate trimer preparation or the protection liquid B of carrageenan and the preparation of sulfuric acid dextran; sea cucumber behind the compound ion is packed in high temperature resistant, the resistant to elevated temperatures polybag; by protection liquid B behind the sea cucumber weight 1:1-2 adding protection liquid A doubly, suction 10pa-20pa heat seal sealing then.
(4) superhigh pressure technique is handled: vacuum seal is contained the sea cucumber of protect liquid pack in the ultrahigh pressure vessel, put steadily evenly, at first the supercharger pressure value is 15～65Mpa; Flow 5.0～15Mpa/min; Continue pressurization then, the ultrahigh pressure vessel force value was divided into for two stages, and wherein the phase I is 0～300Mpa, constant pressure value 10～15min; Second stage 300～700Mpa, constant pressure value 15～30min; Heating-up temperature is 50 ℃～80 ℃, and be 20～30min heat time heating time, and chilling temperature is 10 ℃～20 ℃; Take out sea cucumber after the pressure relief.
(5) cyclic drying: the sea cucumber that will handle through high pressure technique, evenly be placed in circulation drying baker or the band drier, carry out cyclic drying: first cyclic drying is: 30 ℃-40 ℃ of temperature, air output is 3000～4000kg/h, the cyclic drying time is 8～10h, then the sea cucumber body is turned over a face and puts evenly, and second cyclic drying is: 40 ℃-60 ℃ of temperature, air output is 4000～5000kg/h, and the cyclic drying time is 10～12 hours.The 3rd cyclic drying is 20 ℃～30 ℃ of temperature, and air output is 5000～6000kg/h, and the cyclic drying time is 12～16 hours, then the cyclic drying sea cucumber is taken out, and is cooled to room temperature.
(6) nitrogen-filled packaging: the dried sea-cucumber of ultra-high pressure behind the cyclic drying with high pressure resistant clad aluminum foil packaging bag, with every bag of 300g～1000g dried sea-cucumber, is charged into nitrogen then, and the heat seal sealing gets the dried sea-cucumber of ultra-high pressure finished product.
Described protection liquid A adopts shitosan, sodium phosphate trimer, V
C, pure water is that raw material is formulated, and is formulated by following weight percentages:
Shitosan 2-4%
Sodium phosphate trimer 1-2%
V
C 1-2％
Pure water 93-95%.
Described protection liquid B adopts carrageenan, sulfuric acid dextran, V
C, pure water is that raw material is formulated, and is formulated by following weight percentages:
Carrageenan 1-2%
Sulfuric acid dextran 2-4%
V
C 1-2％
Pure water 93-95%.
Beneficial effect of the present invention is: the present invention from interactional characteristic between sea cucumber protein and the polysaccharide macro-molecular to ionic strength, warm, pressure, pH value sensitiveness, attract each other when molecule enlivens or repel, the strong and weak variation that forms sea cucumber soma recurring structure of active force.Substantially guaranteeing to adopt the superhigh pressure technique preparation under the prerequisite that sea cucumber nutrient material and polysaccharide are not destroyed.At first, the sea cucumber high-temperature processing technology be can remove from, glycosaminoglycan and fucoidin composition in the sea cucumber body better kept through the dried sea-cucumber of superhigh pressure technique preparation.The second, the dried sea-cucumber of superhigh pressure technique preparation, sterilization when having reached the sea cucumber slaking, the enzyme effect of going out strengthens the security of quality under the sea cucumber normality.Three, superhigh pressure technique prepares dried sea-cucumber, and use therein composite anion protection liquid can effectively keep sea cucumber polyanion composition characteristic, strengthens the health care of sea cucumber.Four, adopt superhigh pressure technique to impel sea cucumber before dry, to adopt physics to regulate and make the sea cucumber slaking, remove moisture and make easy preservation, the dried sea-cucumber of instant edible, avoided to boil water repeatedly of conventional processing sea cucumber, add thermal maturation again and cause sea cucumber polysaccharide and protein loss phenomenon, the natural nutritional labeling that can effectively preserve the sea cucumber body.Five, adopt the dried sea-cucumber of superhigh pressure technique preparation, can keep the former form of sea cucumber, the sea cucumber of production to have former color and luster, former nutrition, moisture is low, anti-moisture regain, the anti-accumulation of salt in the surface soil, the characteristics of resistance type.
The specific embodiment
Embodiment 1
Get the fresh and alive extra large stichopus japonicus of 200kg, cut the 15mm openning open from the sea cucumber belly, pick out internal organ, clean the sea cucumber open interior with drinkable water, get sea cucumber 120kg, sea cucumber cleared-out skin rate is 60%.Then the 120kg sea cucumber is placed in the stainless cylinder of steel of 500L, add the 380kg drinkable water, regulating water temperature is 16 ℃, the immersion desalination is pulled out after 10 hours to drench and is removed excessive moisture, desalination sea cucumber 120kg. packs the 120kg sea cucumber in the 500L Stainless Steel Vacuum reactor again, add 3 times of 2% sulfuric acid dextran solution 360kg of sea cucumber weight, the hermetically sealed can mouth, the breakdown vavuum pump vacuumizes 100pa, 40 ℃ of Steam Heating, carry out the compound 6h of anion make sea cucumber fully molten with the sulfuric acid dextran solution in, remove vacuum, get sea cucumber.Get the compound plastic bag of 3000ml, the sea cucumber behind the 120kg composite anion is pressed 120 bags of every packed 1000g packing.Preparation protection liquid is got shitosan 2400g, sodium phosphate trimer 2400g, V then
C1200g; pure water 114kg heats after stirring 80 ℃, all gets 120kg protection liquid after the dissolving; add by sea cucumber weight 1:1; every bag of interpolation 1000g adds to respectively in 120 sacks, vacuumizes 10pa then, the heat seal sealing; 120 packed 120 bags of protection liquid sea cucumbers are arranged; 120 bags of vacuum seals are contained the sea cucumber of protecting liquid pack in the 300L ultrahigh pressure vessel, put steadily evenly airtight container.At supercharger pressure value 15Mpa; Flow 5.0Mpa/min; Start booster, make ultrahigh pressure vessel pressure, be increased to 300Mpa by 0Mpa, pressurize 10min finishes the phase I superhigh pressure technique and handles, and restarts booster, supercharging value 65Mpa, flow 15Mpa/min makes ultrahigh pressure vessel pressure be pressurized to 700Mpa by 300Mpa, pressurize 30min.In pressurization, start electric heater ultrahigh pressure vessel is heated 50 ℃; constant temperature ℃; keep 30min; be cooled to 10 ℃ with the frozen water cooled containers then; when startup pressure-relief valve pressure relief is zero pressure; untie the ultrahigh pressure vessel discharging opening; taking-up is equipped with the sea cucumber sack and is removed protection liquid; evenly be placed in 30 cubic metres the circulating air drying baker; the first cyclic drying temperature is 30 ℃; air output is 4000kg/h; dry 10h; taking out sea cucumber again in drying baker will also join drying tray after body turns over a face; in sending into drying baker, carry out second cyclic drying; 40 ℃ of temperature, air output are 5000kg/h, change the 3rd cyclic drying behind the dry 12h over to; 20 ℃ of temperature; air output is 6000kg/h, dry 16 hours, then dried sea-cucumber is taken out in drying baker; after being cooled to room temperature; get 30kg, going out yield rate is 25%, and water content is 6% dried sea-cucumber of ultra-high pressure; adopt the clad aluminum foil bag; with the dried sea-cucumber 300g that weighs is one bag, is divided into and adorns 100 bags of dried sea-cucumbers, sets every bag with nitrogen filling packing machine and charges into nitrogen 0.003m
3, in 200 ℃ heat seal seal 100 bags of 30kg finished products of dried sea-cucumber of ultra-high pressure.
Embodiment 2
Get the fresh and alive white stichopus japonicus of 200kg, cut the 25mm openning open, pick out internal organ, clean up, in 18 ℃ drinkable water, soak desalination 6 hours, pull out to drench and do, get the clean white stichopus japonicus of 100k from the sea cucumber belly.Then the white stichopus japonicus of 100kg is placed in the stainless cylinder of steel of 500L, adds the 380kg drinkable water, regulating water temperature is 16 ℃, and the immersion desalination is pulled out after 10 hours to drench and removed excessive moisture, gets desalination sea cucumber 100kg..The white stichopus japonicus of 100kg is thrown in the 500L stainless steel cauldron, add 2 times of 4% sulfuric acid dextran solution of white stichopus japonicus weight, sealing material mouth, the breakdown vavuum pump vacuumizes 200pa, heating 60 ℃ makes white thorn participate in that the sulfuric acid dextran solution is fully fused removed vacuum after 4 hours, and it is standby to take out the white stichopus japonicus of 100kg.Get the compound plastic bag of 3000ml, the sea cucumber behind the 100kg composite anion is pressed 100 bags of every packed 1000g packing.Liquid is protected in preparation then; get carrageenan 4000g; sulfuric acid dextran 8000g; VC2000g; pure water 186kg, after the 80 ℃ of dissolvings of heating the composite protection liquid of super-pressure 200kg, with white stichopus japonicus one bag of 1000g in the high pressure resistant compound plastic bag of packing by weight; add the protection liquid of 2000g again, be sealed to 100 bags in the heat seal of 20pa vacuum.Vacuum seal is contained the white stichopus japonicus of protecting liquid be respectively charged in the 300L ultrahigh pressure vessel for 100 bags and seal, put steadily evenly.At supercharger pressure value 15Mpa; Flow 5.0Mpa/min; Start booster, make ultrahigh pressure vessel pressure, be increased to 300Mpa by 0Mpa, pressurize 15min finishes the phase I superhigh pressure technique and handles, and restarts booster, supercharging value 65Mpa, flow 15Mpa/min makes ultrahigh pressure vessel pressure be pressurized to 700Mpa by 300Mpa, pressurize 15min.In pressurization, start electric heater ultrahigh pressure vessel is heated 80 ℃; keep 20min; be cooled to 20 ℃ with the frozen water cooled containers then; when starting the pressure-relief valve pressure relief and being zero pressure, untie the ultrahigh pressure vessel discharging opening, take out and the sea cucumber sack is housed removes protection liquid; evenly be placed in 30 cubic metres the circulating air drying baker; the first cyclic drying temperature is 40 ℃, and air output is 3000kg/h, dry 8h; taking out sea cucumber again in drying baker will also join drying tray after body turns over a face; in sending into drying baker, carry out second cyclic drying, 60 ℃ of temperature, air output is 4000kg/h; change the 3rd cyclic drying over to behind the dry 10h; 30 ℃ of temperature, air output are 5000kg/h, dry 12 hours; then dried sea-cucumber is taken out in drying baker; after being cooled to room temperature, get 25kg, going out yield rate is 25%; water content is 6% dried sea-cucumber of ultra-high pressure; adopting the clad aluminum foil bag, is one bag with the dried sea-cucumber 1000g that weighs, and sets every bag with nitrogen filling packing machine and charges into nitrogen 0.003m
3, in 200 ℃ heat seal seal 25 bags of 25kg finished products of dried sea-cucumber of ultra-high pressure.
Claims (3)
1, a kind of preparation method of dried sea-cucumber of ultra-high pressure is characterized in that being finished by following step:
(1) sea cucumber preprocessing: cut fresh and alive sea cucumbers the openning of 15-25mm open in the middle of the belly, reject internal organ, clean up, be seated in 16 ℃-18 ℃ the drinkable water and soak desalination 6-10h, pull out to drench and do;
(2) compound ion: adopt the Stainless Steel Vacuum reactor, pretreated sea cucumber is thrown in reactor, add sea cucumber weight 1:2-3 2-4% sulfuric acid dextran solution doubly, at vacuum 100pa-200pa, 40 ℃-60 ℃ of temperature, carried out the compound 4-6 of anion hour, and removed vacuum again, the taking-up sea cucumber is standby;
(3) composite protection liquid: adopt the protection liquid A of shitosan and sodium phosphate trimer preparation or the protection liquid B of carrageenan and the preparation of sulfuric acid dextran, sea cucumber behind the compound ion is packed in high temperature resistant, the resistant to elevated temperatures polybag, by protection liquid B behind the sea cucumber weight 1:1-2 adding protection liquid A doubly, suction 10pa-20pa heat seal sealing then;
(4) superhigh pressure technique is handled: vacuum seal is contained the sea cucumber of protect liquid pack in the ultrahigh pressure vessel, put steadily evenly, at first the supercharger pressure value is 15～65Mpa; Flow 5.0～15Mpa/min; Continue pressurization then, the ultrahigh pressure vessel force value was divided into for two stages, and wherein the phase I is 0～300Mpa, constant pressure value 10～15min; Second stage 300～700Mpa, constant pressure value 15～30min; Heating-up temperature is 50 ℃～80 ℃, and be 20～30min heat time heating time, and chilling temperature is 10 ℃～20 ℃; Take out sea cucumber after the pressure relief;
(5) cyclic drying: the sea cucumber that will handle through high pressure technique, evenly be placed in circulation drying baker or the band drier, carry out cyclic drying: first cyclic drying is: 30 ℃-40 ℃ of temperature, air output is 3000～4000kg/h, the cyclic drying time is 8～10h, then the sea cucumber body being turned over a face puts evenly, second cyclic drying is: 40 ℃-60 ℃ of temperature, air output is 4000～5000kg/h, and the cyclic drying time is 10～12 hours, and the 3rd cyclic drying is 20 ℃～30 ℃ of temperature, air output is 5000～6000kg/h, the cyclic drying time is 12～16 hours, then the cyclic drying sea cucumber is taken out, and is cooled to room temperature;
(6) nitrogen-filled packaging: the dried sea-cucumber of ultra-high pressure behind the cyclic drying with high pressure resistant clad aluminum foil packaging bag, with every bag of 300g～1000g dried sea-cucumber, is charged into nitrogen then, and the heat seal sealing gets the dried sea-cucumber of ultra-high pressure finished product.
2, the preparation method of dried sea-cucumber of ultra-high pressure as claimed in claim 1 is characterized in that: described protection liquid A adopts shitosan, sodium phosphate trimer, V
C, pure water is that raw material is formulated, and is formulated by following weight percentages:
Shitosan 2-4%
Sodium phosphate trimer 1-2%
V
C 1-2％
Pure water 93-95%.
3, the preparation method of dried sea-cucumber of ultra-high pressure as claimed in claim 1 is characterized in that: described protection liquid B adopts carrageenan, sulfuric acid dextran, V
C, pure water is that raw material is formulated, and is formulated by following weight percentages:
Carrageenan 1-2%
Sulfuric acid dextran 2-4%
V
C 1-2％
Pure water 93-95%.
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Cited By (9)
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| CN101703238B (en) * | 2009-11-05 | 2012-11-28 | 大连海晏堂生物有限公司 | Sea-cucumber chitosan capsules and preparation method thereof |
| CN102928314A (en) * | 2012-11-20 | 2013-02-13 | 中国水产科学研究院黄海水产研究所 | Measurement method for external dopants in dried sea cucumber |
| CN103598626A (en) * | 2013-11-22 | 2014-02-26 | 大连爱冬水产食品有限公司 | Production method for delicious instant sea cucumbers |
| CN103755824A (en) * | 2013-12-26 | 2014-04-30 | 青岛福创环境科技有限公司 | Process for extracting fucoidin from alga by enzyme method |
| CN104289156A (en) * | 2014-10-27 | 2015-01-21 | 甘肃中医学院 | Method for softening traditional Chinese medicinal material before slicing |
| CN104892785A (en) * | 2015-05-29 | 2015-09-09 | 湖南尔康制药股份有限公司 | Extraction method of seaweed polysaccharide |
| CN105475890A (en) * | 2015-12-30 | 2016-04-13 | 山东好当家海洋发展股份有限公司 | Preparation method of salted dried sea cucumber |
| CN106136019A (en) * | 2016-05-18 | 2016-11-23 | 彝良山益宝生物科技有限公司 | A kind of preparation method of superhigh pressure fresh-keeping Rhizoma Gastrodiae |
| CN106359526A (en) * | 2016-11-08 | 2017-02-01 | 大连国富水产食品有限公司 | Sea cucumber processing process |
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| CN101002577A (en) * | 2006-11-16 | 2007-07-25 | 天津市华泰森淼生物工程技术有限公司 | Novel method for preserving and processing sea cuumber |
| CN101209115A (en) * | 2006-12-25 | 2008-07-02 | 邓洁 | Method and application for processing fresh sea cucumber by low temperature ultra-high pressure freeze drying micro-powder technique |
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- 2008-11-14 CN CN2008101621742A patent/CN101411522B/en not_active Expired - Fee Related
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101703238B (en) * | 2009-11-05 | 2012-11-28 | 大连海晏堂生物有限公司 | Sea-cucumber chitosan capsules and preparation method thereof |
| CN102928314A (en) * | 2012-11-20 | 2013-02-13 | 中国水产科学研究院黄海水产研究所 | Measurement method for external dopants in dried sea cucumber |
| CN103598626A (en) * | 2013-11-22 | 2014-02-26 | 大连爱冬水产食品有限公司 | Production method for delicious instant sea cucumbers |
| CN103755824A (en) * | 2013-12-26 | 2014-04-30 | 青岛福创环境科技有限公司 | Process for extracting fucoidin from alga by enzyme method |
| CN103755824B (en) * | 2013-12-26 | 2016-01-20 | 青岛福创环境科技有限公司 | The technique of fucoidin in a kind of Enzymatic Extraction marine alga |
| CN104289156A (en) * | 2014-10-27 | 2015-01-21 | 甘肃中医学院 | Method for softening traditional Chinese medicinal material before slicing |
| CN104892785A (en) * | 2015-05-29 | 2015-09-09 | 湖南尔康制药股份有限公司 | Extraction method of seaweed polysaccharide |
| CN104892785B (en) * | 2015-05-29 | 2017-07-07 | 湖南尔康制药股份有限公司 | A kind of extracting method of algal polysaccharides |
| CN105475890A (en) * | 2015-12-30 | 2016-04-13 | 山东好当家海洋发展股份有限公司 | Preparation method of salted dried sea cucumber |
| CN106136019A (en) * | 2016-05-18 | 2016-11-23 | 彝良山益宝生物科技有限公司 | A kind of preparation method of superhigh pressure fresh-keeping Rhizoma Gastrodiae |
| CN106359526A (en) * | 2016-11-08 | 2017-02-01 | 大连国富水产食品有限公司 | Sea cucumber processing process |
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